Laboratory

...

Quality control

The presence of its own laboratory allows for multi-stage monitoring of production processes and guarantees first-class quality of the lubricants produced.

The high-tech and modern laboratory for the analysis of petroleum products of LLC "Krokus" was established in 2021. The laboratory is equipped with modern calibrated measuring instruments, certified testing equipment, and auxiliary equipment corresponding to the research objects and the list of determined indicators. The laboratory staff is composed of specialists with the appropriate professional training and experience in conducting tests. Laboratory employees continuously improve their professional level, mastering new testing methods and modern laboratory equipment.


The laboratory's tasks include:

  • —  Quality control of incoming raw materials
  • —  Intermediate control of stages of the production process
  • —  Quality control of finished products
  • —  Scientific research on the development of new products
  • —  Research on the implementation of new formulations and production technologies.

 

Laboratory services:

Indicator name

Testing method

Kinematic viscosity

GOST 33

ASTM D 445         

Acid number

GOST 5985

GOST 5985

GOST 31933

GOST 11362 p. 10.2

Corrosion test

GOST 2917

Corrosive action on steel plates

GOST 25821

Viscosity stability after oil sonication in ultrasonic equipment

GOST 6794

Oil film quality

GOST 6794

Content of water-soluble acids and alkalis

GOST 6307

Mass fraction of mechanical impurities

GOST 10577

Change in mass of rubber after being kept in oil

GOST 9.030

Mass fraction of water

GOST 2477

Flash point determined in an open cup

GOST 4333

ASTM D 92

Pour point

GOST 20287

Density

GOST 3900

GOST R 51069

Tribological characteristics determined on a four-ball tribometer:

GOST 9490

- wear rate (Di)

- flash point index (Iz)

- scuffing load (Rs)

- critical load (Rk)

Viscosity index

GOST 25371

ASTM D 2270

Acid number

GOST 5985

Ash content

GOST 1461

Thermo-oxidative stability:

GOST 11063

- mass fraction of sediment in oxidized oil

- change in viscosity

Oxidation stability:

GOST 981

- mass fraction of sediment

- acid number

Thermo-oxidative stability and corrosive activity:

GOST 20944

- kinematic viscosity after oxidation

GOST 33

- acid number after oxidation

GOST 5985

Mass fraction of zinc

GOST 13538   

Mass fraction of barium

Mass fraction of calcium

Mass fraction of mechanical impurities

GOST 6370

Mass fraction of mechanical impurities

GOST 25821

Mechanical impurities visually

TU 6-00-5763445-10-89

Content of mechanical impurities

GOST 6479

Sulfated ash

GOST 12417

Water content

GOST 1547     

Odor

Organoleptically   

Flash point determined in a closed cup

ASTM D 93  

Cleanliness class

GOST 17216

Thermo-oxidative stability. Properties of oil after oxidation:

GOST 23797

- kinematic viscosity after oxidation, at temperature:

- 100 ºC

- 50 ºC

- minus 15 ºC

- minus 40 ºC

- acid number after oxidation

- mass fraction of sediment after oxidation

- corrosiveness on metal plates

Thermo-oxidative stability and corrosive activity at 200 ºC.  Properties of oil after oxidation:

GOST 20944

- kinematic viscosity after oxidation, at temperature:

- 20 °C

- 50 °C

- minus 60 °C

- acid number after oxidation

- corrosiveness on metal plates

Alkalinity number

GOST 11362

ASTM D 2896

Foaming /  Foam stability

GOST 25821

ASTM D 892

Tendency to foam formation /  Foam stability

GOST 23652 p. 5.5

Demulsifying properties:

GOST ISO 6614

- emulsion separation time

- volume of layers:

- oil

- water

- emulsion

Saponification number

GOST 17362

pH value

GOST 25821

GOST 22567.5

pH of emulsion

GOST 6243

Emulsion stability

GOST 5702

Acid number

GOST 31933

Flash point determined in a closed cup

GOST 6356

Crystallization temperature

GOST 28084

Color on CN colorimeter

GOST 20284